Hostname: page-component-55f67697df-xq6d9 Total loading time: 0 Render date: 2025-05-12T00:10:23.217Z Has data issue: false hasContentIssue false
  • English
  • Français

VULCAN: A “hammer” for high-temperature materials research

Published online by Cambridge University Press:  06 November 2019

Ke An ,
Yan Chen  and
Alexandru D. Stoica
Ke An
Affiliation:
Spallation Neutron Source, Oak Ridge National Laboratory, USA; [email protected]
Yan Chen
Affiliation:
Spallation Neutron Source, Oak Ridge National Laboratory, USA; [email protected]
Alexandru D. Stoica
Affiliation:
Spallation Neutron Source, Oak Ridge National Laboratory, USA; [email protected]
Get access

Abstract

Understanding changes in chemistry, microstructure, and physical properties during synthesis, processing, testing, and even service is vital for materials design and performance. Compared to traditional postmortem material characterization tools, in situ crystallographic characterization can provide considerable data and information on evolution of chemistry, dislocations, twinning, texture, and strains when a material is under external stimuli. Neutrons especially are able to probe material bulk properties and behaviors in extreme environments, thanks to their deep penetrating power and unique sensitivity to differentiate elements from lightweight to transition-metal atoms. In this article, we introduce and describe a diffractometer named VULCAN, which is located at Oak Ridge National Laboratory. This represents a powerful tool to understand materials properties and behaviors under complex environments, in particular, at high temperatures.

Type
High-Temperature Materials for Structural Applications
Information
MRS Bulletin , Volume 44 , Issue 11: High-temperature Materials for Structural Applications , November 2019 , pp. 878 - 885
Copyright
Copyright © Materials Research Society 2019 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Article purchase

Temporarily unavailable

References

An, K., Skorpenske, H.D., Stoica, A.D., Ma, D., Wang, X.-L., Metall. Mater. Trans. A 42a, 95 (2011).10.1007/s11661-010-0495-9CrossRefGoogle Scholar
Calder, S., An, K., Boehler, R., Dela Cruz, C.R., Frontzek, M.D., Guthrie, M., Haberl, B., Huq, A., Kimber, S.A.J., Liu, J., Molaison, J.J., Neuefeind, J., Page, K., dos Santos, A.M., Taddei, K.M., Tulk, C., Tucker, M.G., Rev. Sci. Instrum. 89, 92701 (2018).10.1063/1.5033906CrossRefGoogle Scholar
An, K., Armitage, D.P., Yu, Z., Dickson, R.W., Mills, R.A., Feng, Z., Skorpenske, H.D., Rev. Sci. Instrum. 89, 92901 (2018).10.1063/1.5033566CrossRefGoogle Scholar
Mauro, N.A., Vogt, A.J., Derendorf, K.S., Johnson, M.L., Rustan, G.E., Quirinale, D.G., Kreyssig, A., Lokshin, K.A., Neuefeind, J.C., An, K., Wang, X.-L., Goldman, A.I., Egami, T., Kelton, K.F., Rev. Sci. Instrum. 87, 13904 (2016).10.1063/1.4939194CrossRefGoogle Scholar
Granroth, G.E., An, K., Smith, H.L., Whitfield, P., Neuefeind, J.C., Lee, J., Zhou, W., Sedov, V.N., Peterson, P.F., Parizzi, A., Skorpenske, H., Hartman, S.M., Huq, A., Abernathy, D.L., J. Appl. Crystallogr. 51, 616 (2018).10.1107/S1600576718004727CrossRefGoogle Scholar
An, K., VDRIVE-Data Reduction and Interactive Visualization Software for Event Mode Neutron Diffraction (Oak Ridge National Laboratory, Oak Ridge, TN, 2012).Google Scholar
Chen, Y., Yang, L., Ren, F., An, K., Sci. Rep. 4, 5179 (2014).10.1038/srep05179CrossRefGoogle Scholar
Yu, D., Chen, Y., Huang, L., An, K., Crystals 8, (2018).Google Scholar
Yu, Z.Z., Feng, Z., An, K., Zhang, W., Specht, E.D., Chen, J., Wang, X.-L., David, S., “In Situ Neutron Diffraction Study of Nonequilibrium Phase Transformation in Advanced High-Strength Steels,” Proc. 9th Int. Conf. Trends Weld. Res. (ASM International, Materials Park, OH, 2013), pp. 506–509.Google Scholar
Chen, Y., Rangasamy, E., Lang, C.D., An, K., Chem. Mater. 27, 5491 (2015).CrossRefGoogle Scholar
Wang, S.W., Chen, Y., Fang, S., Zhang, L., Tang, M., An, K., Brinkman, K.S., Chen, F., Chem. Mater. 26, 2021 (2014).10.1021/cm403684bCrossRefGoogle Scholar
Cai, L., Liu, Z.C., An, K., Liang, C.D., J. Mater. Chem. A 1, 6908 (2013).10.1039/c3ta00145hCrossRefGoogle Scholar
Chen, Y., Cheng, Y., Li, J., Feygenson, M., Heller, W.T., Liang, C., Adv. Energy Mater. 7, (2017), https://doi.org/10.1002/aenm.20177002.Google Scholar
Radecka, A., Coakley, J., Jones, I.P., Rugg, D., Lindley, T.C., Dye, D., Mater. Sci. Eng. A 650, 28 (2016).10.1016/j.msea.2015.09.070CrossRefGoogle Scholar
Stoica, G.M., Dessieux, L.L., Stoica, A.D., Vogel, S.C., Muralidharan, G., Radhakrishnan, B., Gorti, S.B., An, K., Ma, D., Wang, X.-L., Quantum Beam Sci . 2, 17 (2018).10.3390/qubs2030017CrossRefGoogle Scholar
Stoica, G.M., Stoica, A.D., Miller, M.K., Ma, D., Nat. Commun. 5, 5178 (2014).10.1038/ncomms6178CrossRefGoogle Scholar
Lugovy, M., Aman, A., Chen, Y., Orlovskaya, N., Kuebler, J., Graule, T., Reece, M.J., Ma, D., Stoica, A.D., An, K., J. Appl. Phys. 116, 13504 (2014).10.1063/1.4884336CrossRefGoogle Scholar
Stoica, G.M., Stoica, A.D., An, K., Ma, D., Vogel, S.C., Carpenter, J.S., Wang, X.-L., J. Appl. Crystallogr. 47, 2019 (2014).10.1107/S1600576714023036CrossRefGoogle Scholar
Liu, T.K., Wu, Z., Stoica, A.D., Xie, Q., Wu, W., Gao, Y.F., Bei, H., An, K., Mater. Des. 131, 419 (2017).10.1016/j.matdes.2017.06.039CrossRefGoogle Scholar
Yu, D., Bei, H., Chen, Y., George, E.P., An, K., Scr. Mater. 84–85, 59 (2014).CrossRefGoogle Scholar
Xie, Q., Chen, Y., Yang, P., Zhao, Z., Wang, Y.D., An, K., Scr. Mater. 150, 168 (2018).10.1016/j.scriptamat.2018.03.017CrossRefGoogle Scholar
de Bellefon, G.M., Gussev, M.N., Stoica, A.D., van Duysen, J.C., Sridharan, K., Scr. Mater . 157, 162 (2018).CrossRefGoogle Scholar
Wu, W., An, K., Huang, L., Lee, S.Y., Liaw, P.K., Scr. Mater. 69, 358 (2013).10.1016/j.scriptamat.2013.05.008CrossRefGoogle Scholar
Wu, W., Qiao, H., An, K., Guo, X., Wu, P., Liaw, P.K., Int. J. Plast. 62, 105 (2014).10.1016/j.ijplas.2014.07.005CrossRefGoogle Scholar
Wu, W., Liaw, P.K., An, K., Acta Mater . 85, 343 (2015).CrossRefGoogle Scholar
Xie, Q., Pei, Z., Liang, J., Yu, D., Zhao, Z., Yang, P., Li, R., Eisenbach, M., An, K., Acta Mater . 161, 273 (2018).10.1016/j.actamat.2018.09.020CrossRefGoogle Scholar
Yu, D., An, K., Chen, Y., Chen, X., Scr. Mater. 89, 45 (2014).10.1016/j.scriptamat.2014.06.021CrossRefGoogle Scholar
Fu, S., Bei, H., Chen, Y., Liu, T.K., Yu, D., An, K., Mater. Res. Lett. 6, 620 (2018).CrossRefGoogle Scholar
Wang, D.M., Chen, Y., Mu, J., Zhu, Z.W., Zhang, H.F., Wang, Y.D., An, K., Scr. Mater. 153, 118 (2018).10.1016/j.scriptamat.2018.05.012CrossRefGoogle Scholar
Benafan, O., Noebe, R.D., Padula, S.A. II, Gaydosh, D.J., Lerch, B.A., Garg, A., Bigelow, G.S., An, K., Vaidyanathan, R., Scr. Mater. 68, 571 (2013).10.1016/j.scriptamat.2012.11.042CrossRefGoogle Scholar
Yang, H., Yu, D., Chen, Y., Mu, J., Wang, Y.D., An, K., Mater. Sci. Eng. A 680, 324 (2017).10.1016/j.msea.2016.10.078CrossRefGoogle Scholar
Rauch, H.A., Chen, Y., An, K., Yu, H.Z., Acta Mater . 168, 362 (2019).10.1016/j.actamat.2019.02.028CrossRefGoogle Scholar
Wu, Y., Ma, D., Li, Q.K., Stoica, A.D., Song, W.L., Wang, H., Liu, X.J., Stoica, G.M., Wang, G.Y., An, K., Wang, X.L., Li, M., Lu, Z.P., Acta Mater . 124, 478 (2017).10.1016/j.actamat.2016.11.029CrossRefGoogle Scholar
Wang, D.M., Mu, J., Chen, Y., Qi, Y., Wu, W., Wang, Y., Xu, H., Zhang, H., An, K., J. Alloys Compd. 696, 1096 (2017).10.1016/j.jallcom.2016.12.020CrossRefGoogle Scholar
Maurya, D., Murayama, M., Pramanick, A., Reynolds, W.T. Jr., An, K., Priya, S., J. Appl. Phys. 113, 114101 (2013).10.1063/1.4792729CrossRefGoogle Scholar
Wang, X.L., An, K., Cai, L., Feng, Z., Nagler, S.E., Daniel, C., Rhodes, K.J., Stoica, A.D., Skorpenske, H.D., Liang, C., Zhang, W., Kim, J., Qi, Y., Harris, S.J., Sci. Rep. 2, 747 (2012).10.1038/srep00747CrossRefGoogle Scholar
Cai, L., An, K., Feng, Z.L., Liang, C.D., Harris, S.J., J. Power Sources 236, 163 (2013).10.1016/j.jpowsour.2013.02.066CrossRefGoogle Scholar
Liu, H.D., Fell, C.R., An, K., Cai, L., Meng, Y.S., J. Power Sources 240, 772 (2013).10.1016/j.jpowsour.2013.04.149CrossRefGoogle Scholar
Chen, Y., Rangasamy, E., dela Cruz, C.R., Liang, C.D., An, K., J. Mater. Chem. A 3, 22868 (2015).10.1039/C5TA04902DCrossRefGoogle Scholar
Xu, G.L., Qin, Y., Ren, Y., Cai, L., An, K., Amine, K., Chen, Z., J. Mater. Chem. A 3, 13031 (2015).10.1039/C5TA02522BCrossRefGoogle Scholar
Yang, T., Matthews, A.H., Xu, N., Chen, Y., An, K., Ma, D., Huang, K., ACS Appl. Mater. Interfaces 10, 35984 (2018).10.1021/acsami.8b12943CrossRefGoogle Scholar
Yang, T., Wang, J., Chen, Y., An, K., Ma, D., Vogt, T., Huang, K., ACS Appl. Mater. Interfaces 9, 34855 (2017).10.1021/acsami.7b08697CrossRefGoogle ScholarPubMed
Ren, F., Schmidt, R., Keum, J.K., Qian, B., Case, E.D., Littrell, K.C., An, K., Appl. Phys. Lett. 109, 81903 (2016).10.1063/1.4961677CrossRefGoogle Scholar
Ren, F., Schmidt, R., Case, E.D., An, K., J. Electron. Mater. 46, 2604 (2017).10.1007/s11664-016-4802-0CrossRefGoogle Scholar
Yeh, J.W., Chen, S.-K., Lin, S.-J., Gan, J.-Y., Chin, T.-S., Shun, T.-T., Tsau, C.-H., Chang, S.-Y., Adv. Eng. Mater. 6, 299 (2004).10.1002/adem.200300567CrossRefGoogle Scholar
Lee, C., Song, G., Gao, M.C., Feng, R., Chen, P., Brechtl, J., Chen, Y., An, K., Guo, W., Poplawsky, J.D., Li, S., Samaei, A.T., Chen, W., Hu, A., Choo, H., Liaw, P.K., Acta Mater . 160, 158 (2018).CrossRefGoogle Scholar
Wu, Y., Liu, W.H., Wang, X.L., Ma, D., Stoica, A.D., Nieh, T.G., He, Z.B., Lu, Z.P., Appl. Phys. Lett. 104, 051910 (2014).10.1063/1.4863748CrossRefGoogle Scholar
Jin, K., Mu, S., An, K., Porter, W.D., Samolyuk, G.D., Stocks, G.M., Bei, H., Mater. Des. 117, 185 (2017).10.1016/j.matdes.2016.12.079CrossRefGoogle Scholar
Liu, T.K., Gao, Y.F., Bei, H.B., An, K., J. Mater. Res. 33, 3192 (2018).CrossRefGoogle Scholar
Huang, H.L., Wu, Y., He, J., Wang, H., Liu, X., An, K., Wu, W., Adv. Mater. 29, (2017), https://doi.org/10.1002/adma.201701678.Google Scholar
Lei, Z.F., Liu, X., Wu, Y., Wang, H., Jiang, S., Wang, S., Hui, X., Wu, Y., Gault, B., Kontis, P., Raabe, D., Gu, L., Zhang, Q., Chen, H., Wang, H., Liu, J., An, K., Zeng, Q., Nieh, T.-G., Lu, Z., Nature 563, 546 (2018).CrossRefGoogle Scholar
Senkov, O.N., Wilks, G.B., Scott, J.M., Miracle, D.B., Intermetallics 19, 698 (2011).CrossRefGoogle Scholar
Yan, H.Y., Coakley, J., Vorontsov, V.A., Jones, N.G., Stone, H.J., Dye, D., Mater. Sci. Eng. A 613, 201 (2014).CrossRefGoogle Scholar
Huang, S.Y., An, K., Gao, Y., Suzuki, A., Metall. Mater. Trans. A 49a, 740 (2018).CrossRefGoogle Scholar
Coakley, J., Lass, E.A., Ma, D., Frost, M., Seidman, D.N., Dunand, D.C., Stone, H.J., Scr. Mater. 134, 110 (2017).CrossRefGoogle Scholar
Huang, S.Y., Gao, Y., An, K., Zheng, L., Wu, W., Teng, Z., Liaw, P.K., Acta Mater . 83, 137 (2015).CrossRefGoogle Scholar
Coakley, J., Ma, D., Frost, M., Dye, D., Seidman, D.N., Dunand, D.C., Stone, H.J., Acta Mater . 135, 77 (2017).CrossRefGoogle Scholar
Yu, D., An, K., Chen, X., Bei, H., J. Alloys Compd. 656, 481 (2016).CrossRefGoogle Scholar
Coakley, J., Lass, E.A., Ma, D., Frost, M., Stone, H.J., Seidman, D.N., Dunand, D.C., Acta Mater . 136, 118 (2017).CrossRefGoogle Scholar
Aba-Perea, P.E., Pirling, T., Preuss, M., Mater. Des. 110, 925 (2016).CrossRefGoogle Scholar
Thompson, S.M., Bian, L.K., Shamsaei, N., Yadollahi, A., Addit. Manuf. 8, 36 (2015).CrossRefGoogle Scholar
An, K., Yuan, L., Dial, L., Spinelli, I., Stoica, A.D., Gao, Y., Mater. Des. 135, 122 (2017).CrossRefGoogle Scholar
Wang, Z.Q., Denlinger, E., Michaleris, P., Stoica, A.D., Ma, D., Beese, A.M., Mater Des . 113, 169 (2017).CrossRefGoogle Scholar
Ma, D., Stoica, A.D., Wang, Z.Q., Beese, A.M., Mater. Sci. Eng. A 684, 47 (2017).CrossRefGoogle Scholar
Wang, Z.Q., Stoica, A.D., Ma, D., Beese, A.M., Mater. Sci. Eng. A 674, 406 (2016).CrossRefGoogle Scholar
Huang, E.W., Lee, S.Y., Jain, J., Tong, Y., An, K., Tsou, N.-T., Lam, T.-N., Yu, D., Chae, H., Chen, S.-W., Chen, S.-M., Chou, H.-S., Intermetallics 109, 60 (2019).CrossRefGoogle Scholar
Cakmak, E., Kirka, M.M., Watkins, T.R., Cooper, R.C., An, K., Choo, H., Wu, W., Dehoff, R.R., Babu, S.S., Acta Mater . 108, 161 (2016).CrossRefGoogle Scholar
Beese, A.M., Wang, Z.Q., Stoica, A.D., Ma, D., Nat Commun . 9, 2083 (2018).CrossRefGoogle Scholar
Song, G., Lin, J.Y.Y., Bilheux, J.C., Xie, Q., Santodonato, L.J., Molaison, J.J., Skorpenske, H.D., Dos Santos, A.M., Tulk, C.A., An, K., Stoica, A.D., Kirka, M.M., Dehoff, R.R., Tremsin, A.S., Bunn, J., Sochalski-Kolbus, L.M., Bilheux, H.Z., J. Imaging 3, 65 (2017).CrossRefGoogle Scholar
Dehoff, R.R., Kirka, M.M., Sames, W.J., Bilheux, H., Tremsin, A.S., Lowe, L.E., Babu, S.S., Mater. Sci. Tech (London) 31, 931 (2015).CrossRefGoogle Scholar
Watkins, T., Bilheux, H., An, K., Payzant, A., Dehoff, R., Duty, C., Peter, W., Blue, C., Brice, C., Adv. Mater. Proc. 171, 23 (2013).Google Scholar
Champion, M.S., Dean, R.A., Galambos, J.D., Howell, M.P., Plum, M.A., Riemer, B.W., “Progress on the Proton Power Upgrade of the Spallation Neutron Source,” Proc. IPAC (Copenhagen, Denmark, 2017).Google Scholar
Wu, W., Stoica, A.D., Berry, K.D., Frost, M.J., Skorpenske, H.D., An, K., Appl. Phys. Lett. 112, 253501 (2018).CrossRefGoogle Scholar