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Strain and Particle Size of Palladium Metal Powders by Time-of-Flight Neutron Diffraction

Published online by Cambridge University Press:  06 March 2019

A. C. Lawson ,
J. W. Conant ,
C. L. Talcott ,
M. A. David ,
J. Vaninetti ,
J. A. Goldstone ,
A. Williams ,
R. B. Roof ,
R. B. Von Dreele  and
R. L. Hitterman
...Show all authors
A. C. Lawson
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
J. W. Conant
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
C. L. Talcott
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
M. A. David
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
J. Vaninetti
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
J. A. Goldstone
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
A. Williams
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
R. B. Roof
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
R. B. Von Dreele
Affiliation:
Los Alamos Rational Laboratory, Los Alamos, NM 87545
R. L. Hitterman
Affiliation:
Argonne Rational Laboratory, Argonne, IL 60439
J. W. Richardson Jr.
Affiliation:
Argonne Rational Laboratory, Argonne, IL 60439
J. Faber Jr.
Affiliation:
Argonne Rational Laboratory, Argonne, IL 60439
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Abstract

We have determined the strain and particle size for several samples of palladium powder by time-of-flight nrutron powder diffraction on two different diffractometers and by x-ray powder diffraction. The results are compared and found to be in fair agreement. The time-of-flight method gives good enough precision to reveal deficiencies in the simple models used for strain and particle size line broadening.

Type
Research Article
Information
Advances in X-Ray Analysis , Volume 33: Thirty-Eighth Annual Conference on Applications of X-ray Analysis, July 31 - August 4, 1989 , 1989 , pp. 403 - 407
Copyright
Copyright © International Centre for Diffraction Data 1989

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References

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